我们采用水热方法合成了“花状” Ni3(NO3)2(OH)4和 Zn5(OH)8(NO3)2(H2O)2 化合物，并以此为模板得到了具有纳米多孔结构的NiO和ZnO材料，并研究了其光学性能。相关研究结果发表在 CrystEngComm 13 , 1831 (2011)上 论文全文： 2011-CrystEngComm-13-1831.pdf ( a,b,c ) FE-SEM image s of the synthesized Ni3(NO3)2(OH)4 flowers; (d) typical TEM image of the individual flower, (e) HR-TEM image of a flake of flowers, and ( f ) SAED pattern of Ni3(NO3)2(OH)4 flower . ( a, b ) FE-SEM image of microflower synthesized at 150 °C and 0.1M Zn(NO3)2·6H2O in 1 h; ( a ) FE-SEM image of NiO flower (obtained from heating Ni3(NO3)2(OH)4 flowers in air at 400 °C for 3 h); (b) typical TEM image of the individual NiO flower; (c) magnified TEM image of the petal and (d)HR-TEM image of a flake of NiO flowers; ( e ) SAED pattern of NiO flowers . (a, b) FESEM images of ZnO obtained after heating zinc compound in air at 400 o C for 3 h; (c) typical TEM image of a ZnO flake; (d) HRTEM image of a flake of a ZnO microflower and the inset is the SAED pattern of as-synthesized ZnO.
标签: 多孔
